13 Zentrale Universitätseinrichtungen
Permanent URI for this collectionhttps://elib.uni-stuttgart.de/handle/11682/14
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Item Open Access Fire rating of post-installed anchors and rebars(2020) Mahrenholtz, Philipp; Sharma, AkanshuFire safety is a critical performance aspect of construction products, and post-installed anchors and rebars are no exemption in that regard. During their service life, anchors and rebars are subjected to different kinds of load actions, so they have to be qualified and designed for critical safety performance. While the qualification guidelines for static and seismic loading have matured to conclusive requirements over the past two decades, the requirements for determining the resistance to fire are just about to consolidate. This contribution strives to provide clarity on the fire rating of post-installed anchors and rebars. For this, the current status of the regulations, as well as the underlying background, is reviewed after a brief introduction. Typical examples of fire ratings in the field of post-installed anchors and rebars are given, and recent research undertaken to close the last regulative gaps is briefly presented.Item Open Access A novel runtime algorithm for the real-time analysis and detection of unexpected changes in a real-size SHM network with quasi-distributed FBG sensors(2021) Sakiyama, Felipe Isamu H.; Lehmann, Frank; Garrecht, HaraldThe ability to track the structural condition of existing structures is one of the main concerns of bridge owners and operators. In the context of bridge maintenance programs, visual inspection predominates nowadays as the primary source of information. Yet, visual inspections alone are insufficient to satisfy the current needs for safety assessment. From this perspective, extensive research on structural health monitoring has been developed in recent decades. However, the transfer rate from laboratory experiments to real-case applications is still unsatisfactory. This paper addresses the main limitations that slow the deployment and the acceptance of real-size structural health monitoring systems (SHM) and presents a novel real-time analysis algorithm based on random variable correlation for condition monitoring. The proposed algorithm was designed to respond automatically to detect unexpected events, such as local structural failure, within a multitude of random dynamic loads. The results are part of a project on SHM, where a high sensor-count monitoring system based on long-gauge fiber Bragg grating sensors (LGFBG) was installed on a prestressed concrete bridge in Neckarsulm, Germany. The authors also present the data management system developed to handle a large amount of data, and demonstrate the results from one of the implemented post-processing methods, the principal component analysis (PCA). The results showed that the deployed SHM system successfully translates the massive raw data into meaningful information. The proposed real-time analysis algorithm delivers a reliable notification system that allows bridge managers to track unexpected events as a basis for decision-making.Item Open Access Investigations of metallurgical differences in AISI 347 and their influence on deformation and transformation behaviour and resulting fatigue life(2024) Veile, Georg; Regitz, Elen; Smaga, Marek; Weihe, Stefan; Beck, TillmannDue to variations in chemical composition and production processes, homonymous austenitic stainless steels can differ significantly regarding their initial microstructure, metastability, and thus, their fatigue behavior. Microstructural investigations and fatigue tests have been performed in order to evaluate this aspect. Three different batches and production forms of nominally one type of steel AISI 347 were investigated under monotonic tensile tests and cyclic loading under total strain and stress control in low and high cycle fatigue regimes, respectively. The deformation induced α’-martensite formation was investigated globally by means of in situ magnetic measurements and locally using optical light microscopy of color etching of micrographs. The investigation showed that the chemical composition and the different production processes influence the material behavior. In fatigue tests, a higher metastability and thus a higher level of deformation induced α’-martensite pronounced cyclic hardening, resulting in significantly greater endurable stresses in total strain-controlled tests and an increase in fatigue life in stress-controlled tests. For applications of non-destructive-testing, detailed knowledge of a component’s metastability is required. In less metastable batches and for lower stress levels, α’-martensite primarily formed at the plasticization zone of a crack. Furthermore, the formation and nucleation points of α’-martensite were highly dependent on grain size and the presence of δ-ferrite. This study provides valuable insights into the different material behavior of three different batches with the same designation, i.e., AISI 347, due to different manufacturing processes and differences in the chemical composition, metastability, and microstructure.Item Open Access Performance‐Prüfverfahren für den Sulfatwiderstand von Beton(2023) Vollpracht, Anya; Feldrappe, Volkert; Overmann, Steffen; Haufe, Johannes; Ehrenberg, Andreas; Beutel, Ralf; Matschei, ThomasDie aktuellen Normen für die Anwendung von Beton sehen deskriptive Regeln für den Einbau in sulfathaltigen Böden und Grundwässern vor. Diese Vorgehensweise schränkt die Anwendungsmöglichkeiten von neuen Bindemitteln und alternativen Betonrezepturen erheblich ein, da diese Baustoffe eine Zustimmung im Einzelfall oder eine allgemeine bauaufsichtliche Zulassung benötigen. Im Zulassungsbereich steht aktuell für die meisten Bindemittel nur das sehr zeitintensive modifizierte SVA‐Verfahren zur Verfügung, mit dem erst nach 2 Jahren Versuchslaufzeit eine Zulassung erfolgen kann. Es wurde daher ein Performance‐Prüfverfahren erarbeitet, das auf der Prüfung der Zugfestigkeit von in Sulfatlösung gelagerten Betonproben basiert. Das Verfahren wurde anhand von 23 verschiedenen Bindemitteln im Hinblick auf seine Aussagekraft untersucht und Abnahmekriterien vorgeschlagen. Derzeit werden Vergleichsuntersuchungen im Labor mit unterschiedlichen w/z‐Werten durchgeführt und es laufen Auslagerungsversuche in einem Anhydrit‐Bergwerk, wo die Proben einer Sulfatkonzentration von 1500 bis 2000 mg/l ausgesetzt sind. Die Proben wurden im Juli 2018 ausgelagert. Darüber hinaus ist ein Ringversuch in Bearbeitung. In diesem Beitrag wird über die Fortschritte zur Etablierung des Prüfverfahrens berichtet.Item Open Access Compressive fatigue investigation on high-strength and ultra-high-strength concrete within the SPP 2020(2022) Basaldella, Marco; Jentsch, Marvin; Oneschkow, Nadja; Markert, Martin; Lohaus, LudgerThe influence of the compressive strength of concrete on fatigue resistance has not been investigated thoroughly and contradictory results can be found in the literature. To date, the focus of concrete fatigue research has been on the determination of the numbers of cycles to failure. Concerning the fatigue behaviour of high-strength concrete (HPC) and, especially, ultra-high-strength concrete (UHPC), which is described by damage indicators such as strain and stiffness development, little knowledge is available, as well as with respect to the underlying damage mechanisms. This lack of knowledge has led to uncertainties concerning the treatment of high-strength and ultra-high-strength concretes in the fatigue design rules. This paper aims to decrease the lack of knowledge concerning the fatigue behaviour of concrete compositions characterised by a very high strength. Within the priority programme SPP 2020, one HPC and one UHPC subjected to monotonically increasing and cyclic loading were investigated comparatively in terms of their numbers of cycles to failure, as well as the damage indicators strain and stiffness. The results show that the UHPC reaches a higher stiffness and a higher ultimate strain and strength than the HPC. The fatigue investigations reveal that the UHPC can resist a higher number of cycles to failure than the HPC and the damage indicators show an improved fatigue behaviour of the UHPC compared to the HPC.Item Open Access Anisotropy of the tribological performance of periodically oxidated laser-induced periodic surface structures(2023) Onufrijevs, Pavels; Grase, Liga; Padgurskas, Juozas; Rukanskis, Mindaugas; Durena, Ramona; Willer, Dieter; Iesalnieks, Mairis; Lungevics, Janis; Kaupuzs, Jevgenijs; Rukuiža, Raimundas; Kriūkienė, Rita; Hanesch, Yuliya; Speicher, MagdalenaLaser-induced periodic surface structures (LIPSS) enable advanced surface functionalization with broad applications in various fields such as micro- and nanoelectronics, medicine, microbiology, tribology, anti-icing systems, and more. This study demonstrates the possibility of achieving anisotropy in the tribological behavior of C45-grade steel structured by nanosecond laser radiation using the LIPSS method. The lateral surface of the steel roller was irradiated with a pulsed Nd:YAG laser at an optimum intensity I = 870 MW/cm2 for the formation of LIPSS. Two sets of samples were formed with LIPSS that were perpendicular and parallel to the roller’s rotational motion direction. The Raman intensity maps revealed that the LIPSS structure consisted of periodically arranged oxides at the top of hills. At the same time, the valleys of the LIPSS structures were almost not oxidized. These results correlated well with scanning electron microscopy energy dispersive X-ray spectroscopy mapping and atomic force microscopy measurements. A comparison of Raman and X-ray photoelectron spectroscopy spectra revealed that both the magnetite phase and traces of the hematite phase were present on the surface of the samples. Tribological tests were performed in two cycles with periodic changes in the normal clamping force and sliding speed. It was found that the LIPSS structures which were formed perpendicularly to the sliding direction on the roller had a significantly greater impact on the friction processes. Structures oriented perpendicular to the direction of motion had a positive influence on reducing the energy consumption of a friction process as well as increasing the wear resistance compared to LIPSS formed parallel to the direction of motion or ones having a non-texturized surface. Laser texturing to produce LIPSS perpendicular to the direction of motion could be recommended for friction pairs operating under low-load conditions.Item Open Access Microstructure-based lifetime assessment of austenitic steel AISI 347 in view of fatigue, environmental conditions and NDT(2021) Acosta, Ruth; Heckmann, Klaus; Sievers, Jürgen; Schopf, Tim; Bill, Tobias; Starke, Peter; Donnerbauer, Kai; Lücker, Lukas; Walther, Frank; Boller, ChristianThe assessment of metallic materials used in power plants’ piping represents a big challenge due to the thermal transients and the environmental conditions to which they are exposed. At present, a lack of information related to degradation mechanisms in structures and materials is covered by safety factors in its design, and in some cases, the replacement of components is prescribed after a determined period of time without knowledge of the true degree of degradation. In the collaborative project “Microstructure-based assessment of maximum service life of nuclear materials and components exposed to corrosion and fatigue (MibaLeb)”, a methodology for the assessment of materials’ degradation is being developed, which combines the use of NDT techniques for materials characterization, an optimized fatigue lifetime analysis using short time evaluation procedures (STEPs) and numerical simulations. In this investigation, the AISI 347 (X6CrNiNb18-10) is being analyzed at different conditions in order to validate the methodology. Besides microstructural analysis, tensile and fatigue tests, all to characterize the material, a pressurized hot water pipe exposed to a series of flow conditions will be evaluated in terms of full-scale testing as well as prognostic evaluation, where the latter will be based on the materials’ data generated, which should prognose changes in the material’s condition, specifically in a pre-cracked stage. This paper provides an overview of the program, while the more material’s related aspects are presented in the subsequent paper.Item Open Access Analysis of hydrogen-induced changes in the cyclic deformation behavior of AISI 300-series austenitic stainless steels using cyclic indentation testing(2021) Brück, Sven; Blinn, Bastian; Diehl, Katharina; Wissing, Yannick; Müller, Julian; Schwarz, Martina; Christ, Hans-Jürgen; Beck, Tilmann; Staedler, Thorsten; Jiang, Xin; Butz, Benjamin; Weihe, StefanThe locally occurring mechanisms of hydrogen embrittlement significantly influence the fatigue behavior of a material, which was shown in previous research on two different AISI 300-series austenitic stainless steels with different austenite stabilities. In this preliminary work, an enhanced fatigue crack growth as well as changes in crack initiation sites and morphology caused by hydrogen were observed. To further analyze the results obtained in this previous research, in the present work the local cyclic deformation behavior of the material volume was analyzed by using cyclic indentation testing. Moreover, these results were correlated to the local dislocation structures obtained with transmission electron microscopy (TEM) in the vicinity of fatigue cracks. The cyclic indentation tests show a decreased cyclic hardening potential as well as an increased dislocation mobility for the conditions precharged with hydrogen, which correlates to the TEM analysis, revealing courser dislocation cells in the vicinity of the fatigue crack tip. Consequently, the presented results indicate that the hydrogen enhanced localized plasticity (HELP) mechanism leads to accelerated crack growth and change in crack morphology for the materials investigated. In summary, the cyclic indentation tests show a high potential for an analysis of the effects of hydrogen on the local cyclic deformation behavior.Item Open Access Thermodynamic modelling and microstructural study of Z-phase formation in a Ta-alloyed martensitic steel(2021) Riedlsperger, Florian; Gsellmann, Bernadette; Povoden-Karadeniz, Erwin; Tassa, Oriana; Matera, Susanna; Dománková, Mária; Kauffmann, Florian; Kozeschnik, Ernst; Sonderegger, BernhardA thermokinetic computational framework for precipitate transformation simulations in Ta-containing martensitic Z-steels was developed, including Calphad thermodynamics, diffusion mobility data from the literature, and a kinetic parameter setup that considered precipitation sites, interfacial energies and dislocation density evolution. The thermodynamics of Ta-containing subsystems were assessed by atomic solubility data and enthalpies from the literature as well as from the experimental dissolution temperature of Ta-based Z-phase CrTaN obtained from differential scanning calorimetry. Accompanied by a comprehensive transmission electron microscopy analysis of the microstructure, thermokinetic precipitation simulations with a wide-ranging and well-documented set of input parameters were carried out in MatCalc for one sample alloy. A special focus was placed on modelling the transformation of MX into the Z-phase, which was driven by Cr diffusion. The simulation results showed excellent agreement with experimental data in regard to size, number density and chemical composition of the precipitates, showing the usability of the developed thermokinetic simulation framework.Item Open Access Micro-twinning in IN738LC manufactured with laser powder bed fusion(2023) Megahed, Sandra; Krämer, Karl Michael; Kontermann, Christian; Heinze, Christoph; Udoh, Annett; Weihe, Stefan; Oechsner, MatthiasComponents manufactured with Metal Laser Powder Bed Fusion (PBF-LB/M) are built in a layerwise fashion. The PBF-LB/M build orientation affects grain morphology and orientation. Depending on the build orientation, microstructures from equiaxed to textured grains can develop. In the case of a textured microstructure, a clear anisotropy of the mechanical properties affecting short- and long-term mechanical properties can be observed, which must be considered in the component design. Within the scope of this study, the IN738LC tensile and creep properties of PBF-LB/M samples manufactured in 0° (perpendicular to build direction), 45° and 90° (parallel to build direction) build orientations were investigated. While the hot tensile results (at 850 °C) are as expected, where the tensile properties of the 45° build orientation lay between those of 0° and 90°, the creep results (performed at 850 °C and 200 MPa) of the 45° build orientation show the least time to rupture. This study discusses the microstructural reasoning behind the peculiar creep behavior of 45° oriented IN738LC samples and correlates the results to heat-treated microstructures and the solidification conditions of the PBF-LB/M process itself.