02 Fakultät Bau- und Umweltingenieurwissenschaften
Permanent URI for this collectionhttps://elib.uni-stuttgart.de/handle/11682/3
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Item Open Access Comparing methods for permeability computation of porous materials and their limitations(2023) Krach, David; Steeb, HolgerEfficient numerical simulations of fluid flow on the pore scale allow for the numerical estimation of effective material properties of porous media, e.g. intrinsic permeability or tortuosity. These parameters are essential for various applications where hydro‐mechanical properties on larger scales have to be known. Numerical tools based intrinsically on pore scale simulations are known e.g. as Digital Rock Physics in geosciences and have even more and more replaced physical experiments. For these reasons, the validation of numerical methods as well as the establishment of clear limits regarding the application areas play an important role. Here, we compute single‐phase flow through a porous matrix, e.g. irregular sphere packings, sandstones, artificially created thin porous media, on the pore scale. Therefore we implement on the one hand a Smoothed Particle Hydrodynamics algorithm for solving the Navier‐Stokes equations and on the other hand a Finite Difference solver for the Stokes equations. Both methods work directly and seamlessly on voxel data of porous materials which are generated by µXRCT‐scans or by microfluidic experiments that have undergone segmentation and binarization. We compare both solvers from a parallel performance point of view as well as their results for flows in the Darcy regime. In addition, we investigate the limitations of the solvers using the example of a porous material whose pore geometry changes over time and precipitation affects the flow conditions.Item Open Access Parameter identification and validation of shape-memory polymers within the framework of finite strain viscoelasticity(2021) Ghobadi, Ehsan; Shutov, Alexey; Steeb, HolgerShape-Memory Polymers (SMPs) can be stretched to large deformations and recover induced strains when exposed to an appropriate stimulus, such as heat. This emerging class of functional polymers has attracted much interest and found applications in medicine and engineering. Nevertheless, prior to any application, their physical and mechanical properties must be thoroughly studied and understood in order to make predictions or to design structures thereof. In this contribution, the viscoelastic behavior of a polyether-based polyurethane (Estane) and its rate- and temperature-dependent behavior have been studied experimentally and by the mean of simulations. The model-inherent material parameters are identified with the assumption of the thermo-rheological complexity. Here, the numerical results of uni-axial stress relaxations were compared with the associated experiments in conjucation with the Levenberg-Marquard optimization method to determine the parameters of the Prony equation. The ability of the model to simulate the thermo-mechanical properties of Estane was evaluated by data-rich experimental observations on tension and torsion in various temperature ranges. Heterogeneous tests are included into the experimental program to cover a broader spectrum of loading scenarios.Item Open Access Diagnosing hydro-mechanical effects in subsurface fluid flow through fractures(2023) Schmidt, Patrick; Steeb, Holger; Renner, JörgHydro-mechanically induced transient changes in fracture volume elude an analysis of pressure and flow rate transients by conventional diffusion-based models. We used a previously developed fully coupled, inherently non-linear numerical simulation model to demonstrate that harmonic hydraulic excitation of fractures leads to systematic overtones in the response spectrum that can thus be used as a diagnostic criterion for hydro-mechanical interaction. The examination of response spectra, obtained from harmonic testing at four different field sites, for the occurrence of overtones confirmed their potential for the hydro-mechanical characterization of tested reservoirs. A non-dimensional analysis identified relative aperture change as the critical system parameter.Item Open Access The high cycle fatigue testing of High‐Performance Concretes using high frequency excitation(2023) Madadi, Hamid; Steeb, HolgerThe effect of fatigue failure in brittle materials like (ultra) High Performance Concrete (UHPC) due to cyclic loading causes unexpected failure that consequently results in heavy costs in marine and civil structures. To characterize the effect of fatigue, cyclic loading tests are performed, and “the number of cycles to failure” are experimentally determined. One problem with these kinds of tests is that such experimental investigations are potentially expensive, i.e., time‐consuming process since the number of loading cycles could be extremely high. Further, within the different damage phases of the cycling tests, one has no access to the small‐scale, i.e., microscopical evolution of (micro‐)cracks. Additionally, a full characterization of the small‐strain stiffness evolution of the material is challenging. The goal of the research investigation is to combine a (large amplitude) High Cycle Fatigue experiment with a (low amplitude) Dynamic Mechanical Analysis (DMA). Using a setup based on the piezoelectric actuator, the (rate‐dependent) mechanical properties of the material in tangential space, and the failure modes of the material will be examined accurately. The excitation frequency is between 0.01 Hz to 1000 Hz which allows for reducing the experimental investigation time to failure. Further, it allows investigating the effect of frequency on the number of cycles to failure. Firstly, experimental results for HPC and berea sandstone samples will be presented. Harmonic experimental data include (direct) strain measurements in axial and circumferential directions as well as forces in axial directions. In addition, the resulting complex Young's modulus and evolving damage‐like “history” of HPC and berea sandstone specimens will be shown.Item Open Access Experimental evaluation of fluid connectivity in two‐phase flow in porous media during drainage(2022) Vahid Dastjerdi, Samaneh; Karadimitriou, Nikolaos; Hassanizadeh, S. Majid; Steeb, HolgerThis study aims to experimentally investigate the possibility of combining two extended continuum theories for two‐phase flow. One of these theories considers interfacial area as a separate state variable, and the other explicitly discriminates between connected and disconnected phases. This combination enhances our potential to effectively model the apparent hysteresis, which generally dominates two‐phase flow. Using optical microscopy, we perform microfluidic experiments in quasi‐2D artificial porous media for various cyclic displacement processes and boundary conditions. Specifically for a number of sequential drainage processes, with detailed image (post‐)processing, pore‐scale parameters such as the interfacial area between the phases (wetting, non‐wetting, and solid), and local capillary pressure, as well as macroscopic parameters like saturation, are estimated. We show that discriminating between connected and disconnected clusters and the concept of the interfacial area as a separate state variable can be an appropriate way of modeling hysteresis in a two‐phase flow scheme. The drainage datasets of capillary pressure, saturation, and specific interfacial area, are plotted as a surface, given by f (Pc, sw, awn) = 0. These surfaces accommodate all data points within a reasonable experimental error, irrespective of the boundary conditions, as long as the corresponding liquid is connected to its inlet. However, this concept also shows signs of reduced efficiency as a modeling approach in datasets gathered through combining experiments with higher volumetric fluxes. We attribute this observation to the effect of the porous medium geometry on the phase distribution. This yields further elaboration, in which this speculation is thoroughly studied and analyzed.Item Open Access An SPH approach for non-spherical particles immersed in Newtonian fluids(2020) Kijanski, Nadine; Krach, David; Steeb, HolgerSolid particles immersed in a fluid can be found in many engineering, environmental or medical fields. Applications are suspensions, sedimentation processes or procedural processes in the production of medication, food or construction materials. While homogenized behavior of these applications is well understood, contributions in the field of pore-scale fully resolved numerical simulations with non-spherical particles are rare. Using Smoothed Particle Hydrodynamics (SPH) as a simulation framework, we therefore present a modeling approach for Direct Numerical Simulations (DNS) of single-phase fluid containing non-spherically formed solid aggregates. Notable and discussed model specifications are the surface-coupled fluid-solid interaction forces as well as the contact forces between solid aggregates. The focus of this contribution is the numerical modeling approach and its implementation in SPH. Since SPH presents a fully resolved approach, the construction of arbitrary shaped particles is conveniently realizable. After validating our model for single non-spherical particles, we therefore investigate the motion of solid bodies in a Newtonian fluid and their interaction with the surrounding fluid and with other solid bodies by analyzing velocity fields of shear flow with respect to hydromechanical and contact forces. Results show a dependency of the motion and interaction of solid particles on their form and orientation. While spherical particles move to the centerline region, ellipsoidal particles move and rotate due to vortex formation in the fluid flow in between.Item Open Access Experimental methods and imaging for enzymatically induced calcite precipitation in a microfluidic cell(2021) Weinhardt, Felix; Class, Holger; Vahid Dastjerdi, Samaneh; Karadimitriou, Nikolaos; Lee, Dongwon; Steeb, HolgerEnzymatically induced calcite precipitation (EICP) in porous media can be used as an engineering option to achieve precipitation in the pore space, for example, aiming at a targeted sealing of existing flow paths. This is accomplished through a porosity and consequent permeability alteration. A major source of uncertainty in modeling EICP is in the quantitative description of permeability alteration due to precipitation. This report presents methods for investigating experimentally the time‐resolved effects of growing precipitates on porosity and permeability on the pore scale, in a poly‐di‐methyl‐siloxane microfluidic flow cell. These methods include the design and production of the microfluidic cells, the preparation and usage of the chemical solutions, the injection strategy, and the monitoring of pressure drops for given fluxes for the determination of permeability. EICP imaging methods are explained, including optical microscopy and X‐ray microcomputed tomography (XRCT), and the corresponding image processing and analysis. We present and discuss a new experimental procedure using a microfluidic cell, as well as the general perspectives for further experimental and numerical simulation studies on induced calcite precipitation. The results of this study show the enormous benefits and insights achieved by combining both light microscopy and XRCT with hydraulic measurements in microfluidic chips. This allows for a quantitative analysis of the evolution of precipitates with respect to their size and shape, while monitoring their influence on permeability. We consider this to be an improvement of the existing methods in the literature regarding the interpretation of recorded data (pressure, flux, and visualization) during pore morphology alteration.Item Open Access DLP 4D printing of multi‐responsive bilayered structures(2023) Mainik, Philipp; Hsu, Li‐Yun; Zimmer, Claudius W.; Fauser, Dominik; Steeb, Holger; Blasco, EvaAdvances in soft robotics strongly rely on the development and manufacturing of new responsive soft materials. In particular, light‐based 3D printing techniques, and especially, digital light processing (DLP), offer a versatile platform for the fast manufacturing of complex 3D/4D structures with a high spatial resolution. In this work, DLP all‐printed bilayered structures exhibiting reversible and multi‐responsive behavior are presented for the first time. For this purpose, liquid crystal elastomers (LCEs) are used as active layers and combined with a printable non‐responsive elastomer acting as a passive layer. Furthermore, selective light response is incorporated by embedding various organic dyes absorbing light at different regimes in the active layers. An in‐depth characterization of the single materials and printed bilayers demonstrates a reversible and selective response. Last, the versatility of the approach is shown by DLP printing a bilayered complex 3D structure consisting of four different materials (a passive and three different LCE active materials), which exhibit different actuation patterns when irradiated with different wavelengths of light.Item Open Access High‐speed fatigue testing of high‐performance concretes and parallel frequency sweep characterization(2023) Madadi, Hamid; Steeb, HolgerCycling loading of brittle materials like ultra‐high‐performance concrete (UHPC), which is often used in marine and civil structures, results in unexpected failures. When a material is subjected to cyclic loading, its mechanical properties change due to the evolution of (micro‐)fractures often denoted as damage. To better understand the effective material's properties under such kind of fatigue load and to relate the material's properties to the specific time‐dependent loading characteristics, the mechanical response of the material shall be characterized at characteristic harmonic excitations. Therefore, cyclic loading experiments are conducted to determine how the evolution of microfractures, that is, fatigue, affects the material's effective mechanical properties and after how many cycles microfractures further evolve towards meso‐ and macrofractures leading finally to a critical number of cycles to material's failure. The problem with such cyclic fatigue tests is that they are potentially “expensive” to conduct as the number of loading cycles at failure can be extremely high. Moreover, it is not possible to observe and characterize further the evolution of (micro‐)fractures within the different damage phases of the cycling experiment. Further, it is challenging to characterize the material's small‐strain stiffness evolution. In this investigation, a combination of a (high‐amplitude) high‐frequency excitation and a high‐speed fatigue testing approach is used for the high cycle fatigue experiment along with a characterization approach of the material properties using a (low‐amplitude) dynamic mechanical analysis (DMA). The test setup applies harmonic excitations for high and low amplitudes using a high‐voltage piezoelectric actuators. Furthermore, the failure modes of the material will be examined. The excitation frequency 𝑓 for the fatigue test is significantly higher than in classical low- and high-cyclic fatigue approaches, that is, 10 < 𝑓 < 200 Hz, allowing to reduce the overall time of the experimental investigation time to failure. Further, the frequency-dependent number of cycles to failure is studied. Similar to standard DMA, effective complex mechanical properties of the material in tangential space are obtained in frequencies between 0.01 and 1000 Hz; while the observed mechanical properties of these materials change with increasing frequency. In the case of materials' behavior, by increasing the frequency, Young's modulus increases and Poisson's ratio decreases. Experimental fatigue results will be presented for UHPC samples. Harmonic experimental data include (direct) strain measurements in axial and circumferential directions as well as forces in axial directions. In addition, the resulting complex Young's modulus and evolving damage‐like “history” of UHPC will be shown.Item Open Access Influence of humidity on the rheology of thermoresponsive shape memory polymers(2022) Fauser, Dominik; Steeb, HolgerShape Memory Polymers (SMPs) have the inherent ability to maintain a reversible temporary shape and restore a permanent shape under an external trigger. The class of materials has great potential to contribute to smart applications in soft robotics, aerospace, actuation and biomedicine. In these potential application domains, materials are often exposed to large fluctuations due to humidity influences. Therefore, a novel approach is developed to characterize the stronlgy coupled thermal, humidity and time-dependent behavior of polyurethane-based SMP. Weight gain measurements with disk samples of dimension 35 ×35 ×1.5 mm3and linear expansion tests with rectangular samples of dimension 10 ×40 ×1.0 mm3at different relative humidity are carried out to perform the isothermal and isohumid dynamic measurements in thermodynamic equilibrium. The time-temperature superposition is used to characterize and compare the viscoelastic properties at different relative humidity. Concerning effective material properties, a major finding of this investigation is the horizontal shift of the material parameter in the temperature space due to the presence of humidity. Thus, the humidity-dependent material behavior is fully described by a humidity-dependent glass transition temperature. The measured experiments provide a full description of the thermal, humidity and mechanical behavior of SMPs. Graphical abstract