13 Zentrale Universitätseinrichtungen
Permanent URI for this collectionhttps://elib.uni-stuttgart.de/handle/11682/14
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Item Open Access Investigation of oxide layer development of X6CrNiNb18-10 stainless steel exposed to high-temperature water(2024) Veile, Georg; Hirpara, Radhika; Lackmann, Simon; Weihe, StefanThe oxide layer development of X6CrNiNb18-10 (AISI 347) during exposure to high-temperature water has been investigated. Stainless steels are known to form a dual oxide layer in corrosive environments. The secondary Fe-rich oxide layer has no significant protective effect. In contrast, the primary Cr-rich oxide layer is known to reach a stabilized state, protecting the base metal from further oxidation. This study’s purpose was to determine the development of oxide layer dimensions over exposure time using SEM, TEM and EDX line scans. While a parabolic development of Cr in the protective primary layer and Fe in the secondary layer was observed, the dimensions of the Ni layer remained constant. Ni required the presence of a pronounced Fe-rich secondary layer before being able to reside on the outer secondary layer. With increasing immersion time, the Ni element fraction surpassed the Cr element fraction in the secondary layer. Oxide growth on the secondary layer could be observed. After 480 h, nearly the entire surface was covered by the outer oxide layer. In the metal matrix, no depletion of Cr or Ni could be observed over time; however, an increased presence of Cr and Ni in the primary layer was found at the expense of Fe content. The Nb-stabilized stainless steel was subject to the formation of Niobium pentoxide (Nb2O5), with the quantity and magnitude of element fraction increasing over exposure time.Item Open Access Theoretical-numerical investigation of a new approach to reconstruct the temperature field in PBF-LB/M using multispectral process monitoring(2024) May, Lisa; Werz, MartinThe monitoring of additive manufacturing processes such as powder bed fusion enables the detection of several process quantities important to the quality of the built part. In this context, radiation-based monitoring techniques have been used to obtain information about the melt pool and the general temperature distribution on the surface of the powder bed. High temporal and spatial resolution have been achieved at the cost of large storage requirements. This contribution aims to offer an alternative strategy of gaining information about the powder bed’s temperature field with sufficient resolution but with an economical amount of data. The investigated measurement setup uses a spectrometer to detect the spectral radiation intensities emitted by an area enclosing the melt pool and part of its surroundings. An analytical description of this process is presented, which shows that the measured spectral entities can be reconstructed by the Ritz method. It is also shown that the corresponding weighting factors can be physically interpreted as subdomains of constant temperature within the measurement area. Two different test cases are numerically analyzed, showing that the methodology allows for an approximation of the melt pool size while further assumptions remain necessary to reconstruct the actual temperature distribution.Item Open Access Investigation of tool degradation during friction stir welding of hybrid aluminum-steel sheets in a combined butt and overlap joint(2024) Göbel, Robin; Schwertel, Stefanie; Weihe, Stefan; Werz, MartinFriction stir welding, as a solid-state welding technique, is especially suitable for effectively joining high-strength aluminum alloys, as well as for multi-material welds. This research investigates the friction stir welding of thin aluminum and steel sheets, an essential process in the production of hybrid tailor-welded blanks employed in deep drawing applications. Despite its proven advantages, the welding process exhibits variable outcomes concerning formability and joint strength when utilizing an H13 welding tool. To better understand these inconsistencies, multiple welds were performed in this study, joining 1 mm thick steel to 2 mm thick aluminum sheets, with a cumulative length of 7.65 m. The accumulation of material on the welding tool was documented through 3D scanning and weighing. The integrity of the resulting weld seam was analyzed through metallographic sections and X-ray imaging. It was found that the adhering material built up continuously around the tool pin over several welds totaling between 1.5 m and 2.5 m before ultimately detaching. This accretion of material notably affected the welding process, resulting in increased intermixing of steel particles within the aluminum matrix. This research provides detailed insights into the dynamics of friction stir welding in multi-material welds, particularly in the context of tool material interaction and its impact on weld quality.Item Open Access Characterisation of adobe and mud-straw for the restoration and rehabilitation of Persian historical adobe buildings(2024) Hejazi, Bina; Luz, Corinna; Grüner, Friedrich; Frick, Jürgen; Garrecht, HaraldIn the restoration or rehabilitation of traditional buildings, compatible materials with known characteristics must be used. However, the existing literature lacks comprehensive studies on the characterisation of Persian mud-straw plaster, focusing primarily on Persian adobe. Moreover, previous research on Persian adobe has primarily employed XRF and XRD tests, neglecting ion chromatography, moisture sorption isotherm determination, and thermogravimetric analysis with differential scanning calorimetry. Consequently, there is a shortage of information regarding the elemental composition, mineralogical characteristics, moisture sorption behaviour, and thermal properties of Persian mud–straw plaster, as well as Persian adobe bricks. This paper aims to address this research gap by examining historical and new adobe bricks and mud–straw plaster used in Iran, utilising a comprehensive array of analytical techniques. The results from XRF analysis reveal relatively similar chemical compositions across all samples, while XRD analysis indicates predominantly similar mineral phases. Ion chromatography results demonstrate higher conductivity and chloride concentrations in the mud–straw samples than the adobe samples, with higher values for new samples than historical ones. Freshly used straw, clay, or soil may have higher chloride concentrations caused by the arid climate and soil salinisation in the area. Additionally, moisture sorption isotherm determination results show that adobe and mud–straw plaster with a higher salt load of chlorides have significantly higher moisture absorption. The increased straw quantity in the samples increases the moisture content. Furthermore, thermogravimetric analysis and differential scanning calorimetry indicate that, at low heating, adobe and mud–straw plaster lose water due to dehydration, and at high heating, they lose carbon dioxide due to decarboxylation. The comprehensive characterisation of Persian adobe and mud–straw plaster in this study fills a significant gap in the literature and offers invaluable insights for informing restoration and rehabilitation processes, ensuring the compatibility of the materials used.Item Open Access Investigations of metallurgical differences in AISI 347 and their influence on deformation and transformation behaviour and resulting fatigue life(2024) Veile, Georg; Regitz, Elen; Smaga, Marek; Weihe, Stefan; Beck, TillmannDue to variations in chemical composition and production processes, homonymous austenitic stainless steels can differ significantly regarding their initial microstructure, metastability, and thus, their fatigue behavior. Microstructural investigations and fatigue tests have been performed in order to evaluate this aspect. Three different batches and production forms of nominally one type of steel AISI 347 were investigated under monotonic tensile tests and cyclic loading under total strain and stress control in low and high cycle fatigue regimes, respectively. The deformation induced α’-martensite formation was investigated globally by means of in situ magnetic measurements and locally using optical light microscopy of color etching of micrographs. The investigation showed that the chemical composition and the different production processes influence the material behavior. In fatigue tests, a higher metastability and thus a higher level of deformation induced α’-martensite pronounced cyclic hardening, resulting in significantly greater endurable stresses in total strain-controlled tests and an increase in fatigue life in stress-controlled tests. For applications of non-destructive-testing, detailed knowledge of a component’s metastability is required. In less metastable batches and for lower stress levels, α’-martensite primarily formed at the plasticization zone of a crack. Furthermore, the formation and nucleation points of α’-martensite were highly dependent on grain size and the presence of δ-ferrite. This study provides valuable insights into the different material behavior of three different batches with the same designation, i.e., AISI 347, due to different manufacturing processes and differences in the chemical composition, metastability, and microstructure.Item Open Access Impact of wind pressure coefficients on the natural ventilation effectiveness of buildings through simulations(2024) Sakiyama, Nayara Rodrigues Marques; Carlo, Joyce Correna; Sakiyama, Felipe Isamu Harger; Abdessemed, Nadir; Frick, Jürgen; Garrecht, HaraldNatural Ventilation Effectiveness (NVE) is a performance metric that quantifies when outdoor airflows can be used as a cooling strategy to achieve indoor thermal comfort. Based on standard ventilation threshold and building energy simulation (BES) models, the NVE relates available and required airflows to quantify the usefulness of natural ventilation (NV) through design and building evaluation. Since wind is a significant driving force for ventilation, wind pressure coefficients (Cp) represent a critical boundary condition when assessing building airflows. Therefore, this paper investigates the impact of different Cp sources on wind-driven NVE results to see how sensitive the metric is to this variable. For that, an experimental house and a measurement period were used to develop and calibrate the initial BES model. Four Cp sources are considered: an analytical model from the BES software (i), surface-averaged Cp values for building windows that were calculated with Computational Fluid Dynamics (CFD) simulations using OpenFOAM through a cloud-based platform (iia,b,c), and two databases-AIVC (iii) and Tokyo Polytechnic University (TPU) (iv). The results show a variance among the Cp sources, which directly impacts airflow predictions; however, its effect on the performance metric was relatively small. The variation in the NVE outcomes with different Cp’s was 3% at most, and the assessed building could be naturally ventilated around 75% of the investigated time on the first floor and 60% in the ground floor spaces.Item Open Access A universal framework for skill-based cyber-physical production systems(2024) Hossfeld, Max; Wortmann, AndreasIn the vision of smart manufacturing and Industry 4.0, it is vital to automate production processes. There is a significant gap in current practices, where the derivation of production processes from product data still heavily relies on human expertise, leading to inefficiencies and a shortage of skilled labor. This paper proposes a universal framework for skill-based cyber-physical production systems (CPPS) that formalizes production knowledge into machine-processable formats. Key contributions include a novel conceptual model for skill-based production processes and an automated method to derive production plans from high-level CPPS skills for production planning and execution. This framework aims to enhance smart manufacturing by enabling more efficient, transparent, and automated production planning, thereby addressing the critical gap in current manufacturing practices. The framework’s benefits include making production processes explainable, optimizing multi-criteria systems, and eliminating human biases in process selection. A case study illustrates the framework’s application, demonstrating its current capabilities and potential for modern manufacturing.