04 Fakultät Energie-, Verfahrens- und Biotechnik
Permanent URI for this collectionhttps://elib.uni-stuttgart.de/handle/11682/5
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Item Open Access Enhanced processing of regrind as recycling material in single-screw extruders(2021) Thieleke, Philipp; Bonten, ChristianRegrind processing poses challenges for single-screw extruders due to the irregularly shaped particles. For grooved feed zones, the output is lessened by the reduction of bulk density in comparison to virgin material. Simultaneously, the melt temperature increases, reducing the extruder’s process window. Through experimental investigations on a test stand, a novel feed zone geometry (nominal diameter 35 mm) is developed. It aligns the regrind’s specific throughput with that of virgin material. The regrind processing window is essentially increased. As the solids conveying in the novel feed zone cannot be simulated with existing methods, numerical simulations using the discrete element method are performed. Since plastic deformation occurs in the novel feed zone geometry, a new hysteresis contact model is developed. In addition to spheres, the regrind and virgin particles are modeled as superquadrics to better approximate the irregular shape. The new contact model’s simulation results show excellent agreement with experimental compression tests. The throughput of the extruder simulations is considerably underestimated when using spheres to represent the real particles than when using irregularly shaped superquadrics. Corresponding advantages can be seen especially for virgin material.Item Open Access Insights into the processing of recycled carbon fibers via injection molding compounding(2020) Wellekötter, Jochen; Resch, Julia; Baz, Stephan; Gresser, Götz Theo; Bonten, ChristianAlthough fiber-reinforced plastics combine high strength and stiffness with being lightweight, major difficulties arise with high volume production and the return of manufactured parts back into the cycle of materials at the end of their lifecycles. In a novel approach, structural parts were produced from recycled material while utilizing the so-called injection molding compounding process. Recycled fibers and recycled polyamide matrix material were used by blending carbon and matrix fibers into a sliver before processing. Injection molding was then used to produce long fiber-reinforced parts through a direct fiber feed system. Recycled matrix granules were incorporated into the injection molding process by means of an injection molding compounder to investigate their influences on the mechanical properties of the parts. The findings show that the recycled fibers and matrix perform well in standardized tests, although fiber length and fiber content vary significantly and remain below expectations.Item Open Access Comparative analysis of the solid conveying of regrind, virgin and powdery polyolefins in single-screw extrusion(2022) Johann, Kai S.; Reißing, Adrian; Bonten, ChristianThe shape and size of processed materials play a crucial role in the solid conveying characteristics of single-screw extruders. Thus, the increasing amount of plastic regrind leads to new challenges in screw extrusion. This work investigates the conveying behavior of three distinctly different material shapes in an axially as well as a helically grooved solid conveying zone. A uniform virgin polypropylene (PP) granule, an irregularly plate-shaped PP regrind and a powdery polyethylene (PE) are processed at screw speeds up to 1350 rpm. Thereby, frictionally engaged conveying in the grooves is visualized for the utilized powder. Similarly, the virgin granule is subject to forced conveying by interlocking in the grooves. The experimentally determined throughput is furthermore compared to analytical calculations which assume a so-called nut-screw conveying. It is found that these calculations perfectly predict the throughput when processing the virgin granule and the powder in a helically grooved barrel. In contrast, the analytical calculation significantly underestimates the throughput for the regrind. This underestimation is expected to be mainly caused by its plate shape and a difference in bulk density. The actual bulk density in the extruder is probably significantly higher due to both orientation and compaction effects compared to the measured bulk density that is used for the analytical calculation. Additionally, the regrind exhibits a fluctuating throughput due to the non-constant bulk density, which results from an irregular regrind shape and a broad size distribution.Item Open Access Compounding, rheology and numerical simulation of highly filled graphite compounds for potential fuel cell applications(2023) Celik, Alptekin; Willems, Fabian; Tüzün, Mustafa; Marinova, Svetlana; Heyn, Johannes; Fiedler, Markus; Bonten, ChristianHighly filled plastics may offer a suitable solution within the production process for bipolar plates. However, the compounding of conductive additives and the homogeneous mixing of the plastic melt, as well as the accurate prediction of the material behavior, pose a major challenge for polymer engineers. To support the engineering design process of compounding by twin-screw extruders, this present study offers a method to evaluate the achievable mixing quality based on numerical flow simulations. For this purpose, graphite compounds with a filling content of up to 87 wt.-% were successfully produced and characterized rheologically. Based on a particle tracking method, improved element configurations were found for twin-screw compounding. Furthermore, a method to characterize the wall slip ratios of the compounded material system with different filler content is presented, since highly filled material systems often tend to wall slip during processing, which could have a very large influence on accurate prediction. Numerical simulations of the high capillary rheometer were conducted to predict the pressure loss in the capillary. The simulation results show a good agreement and were experimentally validated. In contrast to the expectation, higher filler grades showed only a lower wall slip than compounds with a low graphite content. Despite occurring wall slip effects, the developed flow simulation for the design of slit dies can provide a good prediction for both low and high filling ratios of the graphite compounds.Item Open Access Flow front monitoring in high-pressure resin transfer molding using phased array ultrasonic testing to optimize mold filling simulations(2023) Littner, Linus; Protz, Richard; Kunze, Eckart; Bernhardt, Yannick; Kreutzbruck, Marc; Gude, MaikDuring the production of fiber-reinforced plastics using resin transfer molding (RTM), various characteristic defects and flaws can occur, such as fiber displacement and fiber waviness. Particularly in high-pressure RTM (HP-RTM), fiber misalignments are generated during infiltration by local peaks in the flow rate, leading to a significant reduction in the mechanical properties. To minimize or avoid this effect, the manufacturing process must be well controlled. Simulative approaches allow for a basic design of the mold filling process; however, due to the high number of influencing variables, the real behavior cannot be exactly reproduced. The focus of this work is on flow front monitoring in an HP-RTM mold using phased array ultrasonic testing. By using an established non-destructive testing instrument, the effort required for integration into the manufacturing process can be significantly reduced. For this purpose, investigations were carried out during the production of test specimens composed of glass fiber-reinforced polyurethane resin. Specifically, a phased array ultrasonic probe was used to record individual line scans over the form filling time. Taking into account the specifications of the probe used in these experiments, an area of 48.45 mm was inspected with a spatial resolution of 0.85 mm derived from the pitch. Due to the aperture that had to be applied to improve the signal-to-noise ratio, an averaging of the measured values similar to a moving average over a window of 6.8 mm had to be considered. By varying the orientation of the phased array probe and therefore the orientation of the line scans, it is possible to determine the local flow velocities of the matrix system during mold filling. Furthermore, process simulation studies with locally varying fiber volume contents were carried out. Despite the locally limited measuring range of the monitoring method presented, conclusions about the global flow behavior in a large mold can be drawn by comparing the experimentally determined results with the process simulation studies. The agreement between the measurement and simulation was thus improved by around 70%.Item Open Access Calibration of fiber orientation simulations for LFT : a new approach(2020) Willems, Fabian; Reitinger, Philip; Bonten, ChristianShort fiber reinforced thermoplastics (SFT) are extensively used due to their excellent mechanical properties and low processing costs. Long fiber reinforced thermoplastics (LFT) show an even more interesting property profile and are increasingly used for structural parts. However, their processing by injection molding is not as simple as for SFT, and their anisotropic properties resulting from the fiber microstructure (fiber orientation, length, and concentration) pose a challenge with regard to the engineering design process. To reliably predict the structural mechanical properties of fiber reinforced thermoplastics by means of micromechanical models, it is also necessary to reliable predict the fiber microstructure. Therefore, it is crucial to calibrate the underlying prediction models, such as the fiber orientation model, within the process simulation. In general, these models may be adjusted manually, but this is usually ineffective and time-consuming. To overcome this challenge, a new calibration method was developed to automatically calibrate the fiber orientation model parameters of the injection molding simulation by means of optimization methods. This optimization routine is based on experimentally determined fiber orientation distributions and leads to optimized parameters for the fiber orientation prediction model within a few minutes. To better understand the influence of the model parameters, different versions of the fiber orientation model, as well as process and material influences on the resulting fiber orientation distribution, were investigated. Finally, the developed approach to calibrate the fiber orientation model was compared with a classical approach, a direct optimization of the whole process simulation. Thereby, the new optimization approach shows a calculation time reduced by the factor 15 with comparable error variance.Item Open Access A novel modeling approach for plastics melting within a CFD-DEM framework(2021) Celik, Alptekin; Bonten, Christian; Togni, Riccardo; Kloss, Christoph; Goniva, ChristophExisting three-dimensional modeling approaches to single-screw extrusion can be classified according to the process sections. The discrete element method (DEM) allows describing solids transport in the feed section. The melt flow in the melt section can be calculated by means of computational fluid dynamics (CFD). However, the current state of the art only allows a separate consideration of the respective sections. A joint examination of the process sections still remains challenging. In this study, a novel modeling approach is presented, allowing a joint consideration of solids and melt transport and, beyond that, the formation of melt. For this purpose, the phase transition from the solid to liquid states is modeled for the first time within the framework CFDEMCoupling®, combining CFD and DEM by a novel melting model implemented in this study. In addition, a melting apparatus for the validation of the novel melting model is set up and put into operation. CFD-DEM simulations are carried out in order to calculate the melting rate and are compared to experimental results. A good agreement between the simulation and experimental results is found. From the findings, it can be assumed that the CFD-DEM simulation of single-screw extruder with a joint consideration of the feed and melt section is feasible.Item Open Access Investigation of auxetic structural deformation behavior of PBAT polymers using process and finite element simulation(2023) Schneider, Yanling; Guski, Vinzenz; Sahin, Ahmet O.; Schmauder, Siegfried; Kadkhodapour, Javad; Hufert, Jonas; Grebhardt, Axel; Bonten, ChristianThe current work investigates the auxetic tensile deformation behavior of the inversehoneycomb structure with 5 × 5 cells made of biodegradable poly(butylene adipate-coterephthalate) (PBAT). Fused deposition modeling, an additive manufacturing method, was used to produce such specimens. Residual stress (RS) and warpage, more or less, always exist in such specimens due to their layer-by-layer fabrication, i.e., repeated heating and cooling. The RS influences the auxetic deformation behavior, but its measurement is challenging due to its very fine structure. Instead, the finite-element (FE)-based process simulation realized using an ABAQUS plug-in numerically predicts the RS and warpage. The predicted warpage shows a negligibly slight deviation compared to the design topology. This process simulation also provides the temperature evolution of a small-volume material, revealing the effects of local cyclic heating and cooling. The achieved RS serves as the initial condition for the FE model used to investigate the auxetic tensile behavior. With the outcomes from FE calculation without consideration of the RS, the effect of the RS on the deformation behavior is discussed for the global force–displacement curve, the structural Poisson’s ratio evolution, the deformed structural status, the stress distribution, and the evolution, where the first three and the warpage are also compared with the experimental results. Furthermore, the FE simulation can easily provide the global stress–strain flow curve with the total stress calculated from the elemental stresses.Item Open Access Investigation of the thermal and hydrolytic degradation of polylactide during autoclave foaming(2021) Dreier, Julia; Brütting, Christian; Ruckdäschel, Holger; Altstädt, Volker; Bonten, ChristianPolylactide (PLA) is one of the most important bioplastics worldwide and thus represents a good potential substitute for bead foams made of the fossil-based Polystyrene (PS). However, foaming of PLA comes with a few challenges. One disadvantage of commercially available PLA is its low melt strength and elongation properties, which play an important role in foaming. As a polyester, PLA is also very sensitive to thermal and hydrolytic degradation. Possibilities to overcome these disadvantages can be found in literature, but improving the properties for foaming of PLA as well as the degradation behavior during foaming have not been investigated yet. In this study, reactive extrusion on a twin-screw extruder is used to modify PLA in order to increase the melt strength and to protect it against thermal degradation and hydrolysis. PLA foams are produced in an already known process from the literature and the influence of the modifiers on the properties is estimated. The results show that it is possible to enhance the foaming properties of PLA and to protect it against hydrolysis at the same time.Item Open Access A novel in-line measurement and analysis method of bubble growth-dependent strain and deformation rates during foaming(2024) Schaible, Tobias; Bonten, ChristianBubble growth processes are highly influenced by the elongational viscosity of the blowing agent-loaded polymer melt. Therefore, the elongational viscosity is an important parameter for the development of new polymers for foaming applications, as well as for the prediction of bubble growth processes. Thus, knowledge of the initial expansion and deformation behavior in dependency on the polymer, the blowing agent concentration, and the process conditions is necessary. This study presents a novel method for the in-line observation and analysis of the initial expansion and deformation behavior within the bead foam extrusion process. For this purpose, nitrogen as the blowing agent was injected into the polymer melt (PS and PLA) during the extrusion process. The in-line observation system consists of a borescope equipped with a camera, which was integrated into the water box of an underwater pelletizer. The camera is controlled by a developed trigger by means of angular step signal analysis of a rotary encoder on the cutter shaft of the underwater pelletizer. Thus, images can be taken at any time during the foaming process depending on the cutter position to the die outlet. It is shown that the developed method provides reliable results and that the differences of the initial expansion and deformation behavior during bubble growth can be analyzed in-line in dependency on real foaming process conditions and the type of polymer used.