04 Fakultät Energie-, Verfahrens- und Biotechnik

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    Assessing fatigue life cycles of material X10CrMoVNb9-1 through a combination of experimental and finite element analysis
    (2023) Rahim, Mohammad Ridzwan Bin Abd; Schmauder, Siegfried; Manurung, Yupiter H. P.; Binkele, Peter; Dusza, Ján; Csanádi, Tamás; Ahmad, Meor Iqram Meor; Mat, Muhd Faiz; Dogahe, Kiarash Jamali
    This paper uses a two-scale material modeling approach to investigate fatigue crack initiation and propagation of the material X10CrMoVNb9-1 (P91) under cyclic loading at room temperature. The Voronoi tessellation method was implemented to generate an artificial microstructure model at the microstructure level, and then, the finite element (FE) method was applied to identify different stress distributions. The stress distributions for multiple artificial microstructures was analyzed by using the physically based Tanaka-Mura model to estimate the number of cycles for crack initiation. Considering the prediction of macro-scale and long-term crack formation, the Paris law was utilized in this research. Experimental work on fatigue life with this material was performed, and good agreement was found with the results obtained in FE modeling. The number of cycles for fatigue crack propagation attains up to a maximum of 40% of the final fatigue lifetime with a typical value of 15% in many cases. This physically based two-scale technique significantly advances fatigue research, particularly in power plants, and paves the way for rapid and low-cost virtual material analysis and fatigue resistance analysis in the context of environmental fatigue applications.
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    PFG-NMR studies of ATP diffusion in PEG-DA hydrogels and aqueous solutions of PEG-DA polymers
    (2018) Majer, Günter; Southan, Alexander
    Adenosine triphosphate (ATP) is the major carrier of chemical energy in cells. The diffusion of ATP in hydrogels, which have a structural resemblance to the natural extracellular matrix, is therefore of great importance to understand many biological processes. In continuation of our recent studies of ATP diffusion in poly(ethylene glycol) diacrylate (PEG-DA) hydrogels by pulsed field gradient nuclear magnetic resonance (PFG-NMR), we present precise diffusion measurements of ATP in aqueous solutions of PEG-DA polymers, which are not cross-linked to a three-dimensional network. The dependence of the ATP diffusion on the polymer volume fraction in the hydrogels, φ, was found to be consistent with the predictions of a modified obstruction model or the free volume theory in combination with the sieving behavior of the polymer chains. The present measurements of ATP diffusion in aqueous solutions of the polymers revealed that the diffusion coefficient is determined by φ only, regardless of whether the polymers are cross-linked or not. These results seem to be inconsistent with the free volume model, according to which voids are formed by a statistical redistribution of surrounding molecules, which is expected to occur more frequently in the case of not cross-linked polymers. The present results indicate that ATP diffusion takes place only in the aqueous regions of the systems, with the volume fraction of the polymers, including a solvating water layer, being blocked for the ATP molecules. The solvating water layer increases the effective volume of the polymers by 66%. This modified obstruction model is most appropriate to correctly describe the ATP diffusion in PEG-DA hydrogels.
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    The natural breakup length of a steady capillary jet : application to serial femtosecond crystallography
    (2021) Gañán-Calvo, Alfonso M.; Chapman, Henry N.; Heymann, Michael; Wiedorn, Max O.; Knoska, Juraj; Gañán-Riesco, Braulio; López-Herrera, José M.; Cruz-Mazo, Francisco; Herrada, Miguel A.; Montanero, José M.; Bajt, Saša
    One of the most successful ways to introduce samples in Serial Femtosecond Crystallography has been the use of microscopic capillary liquid jets produced by gas flow focusing, whose length-to-diameter ratio and velocity are essential to fulfill the requirements of the high pulse rates of current XFELs. In this work, we demonstrate the validity of a classical scaling law with two universal constants to calculate that length as a function of the liquid properties and operating conditions. These constants are determined by fitting the scaling law to a large set of experimental and numerical measurements, including previously published data. Both the experimental and numerical jet lengths conform remarkably well to the proposed scaling law. We show that, while a capillary jet is a globally unstable system to linear perturbations above a critical length, its actual and shorter long-term average intact length is determined by the nonlinear perturbations coming from the jet breakup itself. Therefore, this length is determined solely by the properties of the liquid, the average velocity of the liquid and the flow rate expelled. This confirms the very early observations from Smith and Moss 1917, Proc R Soc Lond A Math Phys Eng, 93, 373, to McCarthy and Molloy 1974, Chem Eng J, 7, 1, among others, while it contrasts with the classical conception of temporal stability that attributes the natural breakup length to the jet birth conditions in the ejector or small interactions with the environment.
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    Effects of load forecast deviation on the specification of energy storage systems
    (2023) Emde, Alexander; Märkle, Lisa; Kratzer, Benedikt; Schnell, Felix; Baur, Lukas; Sauer, Alexander
    The liberalization of the German energy market has created opportunities for end-consumers, including industrial companies, to actively participate in the electricity market. By making their energy loads more flexible, consumers can generate additional income and thus save money. Energy storage systems can be utilized to achieve the required flexibility by temporarily storing excess electrical energy in the form of heat, cold, or electricity for later use. This publication focuses on how the dimensionality of energy storage is influenced by load forecasting. The results show that inaccuracies in load forecasting lead to a direct over-dimensioning and thus, a deterioration of the economics of energy storage technologies. Using two scenario cases, it shows on the one hand how important good forecasts are and on the other hand that buffers must be included in the conceptual design in order to be able to compensate for forecast errors.
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    Visualization of the O-X-B mode conversion process with a full-wave code
    (2008) Köhn, Alf; Holzhauer, Eberhard; Stroth, Ulrich
    The O-X-B mode conversion is a process to couple electromagnetic waves into an overdense plasma. At the vicinity of the cutoff, the wave is converted into a Bernstein wave, which is very well absorbed in the plasma without further density cutoff. Therefore, these waves are a promising tool to heat high-density plasmas. The conversion process has been investigated in great detail using a full-wave code, and for the first time, the time-dependent formation of the Bernstein waves has been visualized by using the data obtained with this simulation.
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    Silicon integrated dual-mode interferometer with differential outputs
    (2017) Hoppe, Niklas; Scheck, Pascal; Sweidan, Rami; Diersing, Philipp; Rathgeber, Lotte; Vogel, Wolfgang; Riegger, Benjamin R.; Southan, Alexander; Berroth, Manfred
    The dual-mode interferometer (DMI) is an attractive alternative to Mach-Zehnder interferometers for sensor purposes, achieving sensitivities to refractive index changes close to state-of-the-art. Modern designs on silicon-on-insulator (SOI) platforms offer thermally stable and compact devices with insertion losses of less than 1 dB and high extinction ratios. Compact arrays of multiple DMIs in parallel are easy to fabricate due to the simple structure of the DMI. In this work, the principle of operation of an integrated DMI with differential outputs is presented which allows the unambiguous phase shift detection with a single wavelength measurement, rather than using a wavelength sweep and evaluating the optical output power spectrum. Fluctuating optical input power or varying attenuation due to different analyte concentrations can be compensated by observing the sum of the optical powers at the differential outputs. DMIs with two differential single-mode outputs are fabricated in a 250 nm SOI platform, and corresponding measurements are shown to explain the principle of operation in detail. A comparison of DMIs with the conventional Mach-Zehnder interferometer using the same technology concludes this work.
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    Full-wave modeling of the O-X mode conversion in the Pegasus toroidal experiment
    (2011) Köhn, Alf; Jacquot, Jonathan; Bongard, Michael W.; Gallian, Sara; Hinson, Edward T.; Volpe, Francesco
    The ordinary-extraordinary (O-X) mode conversion is modeled with the aid of a 2D full-wave code in the Pegasus toroidal experiment as a function of the launch angles. It is shown how the shape of the plasma density profile in front of the antenna can significantly influence the mode conversion efficiency and, thus, the generation of electron Bernstein waves (EBWs). It is therefore desirable to control the density profile in front of the antenna for successful operation of an EBW heating and current drive system. On the other hand, the conversion efficiency is shown to be resilient to vertical displacements of the plasma as large as ±10 cm.
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    A consistent and implicit Rhie-Chow interpolation for drag forces in coupled multiphase solvers
    (2021) Hanimann, Lucian; Mangani, Luca; Darwish, Marwan; Casartelli, Ernesto; Vogt, Damian M.
    The use of coupled algorithms for single fluid flow simulation has proven its superiority as opposed to segregated algorithms, especially in terms of robustness and performance. In this paper, the coupled approach is extended for the simulation of multi-fluid flows, using a collocated and pressure-based finite volume discretization technique with a Eulerian-Eulerian model. In this context a key ingredient in this method is extending the Rhie-Chow interpolation technique to account for the unique flow coupling that arises from inter-phase drag. The treatment of this inter-fluid coupling and the fashion in which it interacts with the velocity-pressure solution algorithm is presented in detail and its effect on robustness and accuracy is demonstrated using 2D dilute gas-solid flow test case. The results achieved with this technique show substantial improvement in accuracy and performance when compared to a leading commercial code for a transonic nozzle configuration.